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Notes and references
‡ Crystallographic Data for 3: C90H144Cl14Er8N4O13, T = 293(2) K, Mw
=
3324.47, orthorhombic, space group Aba2, a = 28.632(4), b = 31.254(5),
3
-3
˚
˚
c = 16.142(2) A, V = 14444(4) A , Z = 4, Dc = 1.529 g cm , m(Mo-Ka) =
4.894 mm-1, F(000) = 6392, 12 510 reflections measured, 6617 unique (Rint
=
0.0405) which was used in all calculations. Final R1 = 0.0325 and wR2 =
0.0717 (I > 2s). CCDC 819597. For 4: C90H144Cl14Dy8N4O13, T = 293(2)
K, Mw = 3286.39, orthorhombic, space group Aba2, a = 28.668(6), b =
3
-3
˚
˚
31.282(6), c = 16.199(3) A, V = 14527(5) A , Z = 4, Dc = 1.503 g cm ,
m(Mo-Ka) = 4.359 mm-1, F(000) = 6328, 12 652 reflections measured, 6650
unique (Rint = 0.0819) which was used in all calculations. Final R1 = 0.0490
and wR2 = 0.1078 (I > 2s). CCDC 819598. For 5: C61H89N4, T = 293(2)
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¯
K, Mw = 878.36, triclinic, space group P1, a = 12.937(4),◦b = 13.424(4), c =
˚
17.464(6) A, a = 86.122(5), b = 75.906(5), g = 71.960(5) , V = 2796.9(16)
3
-3
-1
˚
A , Z = 2, Dc = 1.043 g cm , m(Mo-Ka) = 0.060 mm , F(000) = 966, 11 658
reflections measured, 9683 unique (Rint = 0.0346) which was used in all
calculations. Final R1 = 0.0555 and wR2 = 0.1372 (I > 2s). CCDC 819599.
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(4), 819599 (5), 819600 (6).
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¯
For 6: C29H40N2O, T = 293(2) K, Mw = 432.63, triclinic,◦space group P1,
◦
˚
a = 9.177(5), b = 10.603(5), c = 15.394(8) A, a = 85.265(7) , b = 73.552(7) ,
◦
3
-3
˚
g = 66.988(6) , V = 1321.5(11) A , Z = 2, Dc = 1.087 g cm , m(Mo-Ka) =
0.065 mm-1, F(000) = 472, 5497 reflections measured, 4578 unique (Rint
=
0.0651) which was used in all calculations. Final R1 = 0.0932 and wR2 =
0.2381 (I > 2s). CCDC 819590.
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The Royal Society of Chemistry 2012
Dalton Trans., 2012, 41, 357–359 | 359
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