Synthesis p. 474 - 476 (1991)
Update date:2022-07-29
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Chelucci
3-Substituted glutaraldehyde monoacetals 7 have been prepared in 48-58% overall yield, consecutively by the alkylation of nitriles, first with 2-bromo-1,1-diethoxyethane (2) and then with 2-iodomethyl-1,3-dioxolane (4), followed by removal of the cyano group and selective hydrolysis of the diethyl acetal function.
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