Journal of Organic Chemistry p. 8241 - 8244 (1995)
Update date:2022-08-02
Topics:
Zain
Stromberg
Stawinski
A convenient method for the preparation of nucleoside 3'-H-phosphonothioate monoesters from suitably protected nucleoside 3'-H-phosphonates has been developed. It consists of activation of nucleoside H-phosphonates with pivaloyl chloride in the presence of a limited amount of a base followed by treatment with 1,1,1,3,3,3-hexamethyldisilathiane (HMDST).
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