Angewandte Chemie - International Edition p. 3901 - 3904 (2012)
Update date:2022-09-26
Topics:
Bunt, Adam J.
Bailey, Christopher D.
Cons, Benjamin D.
Edwards, Sophie J.
Elsworth, Jon D.
Pheko, Tshepo
Willis, Christine L.
trans-2,8-Dioxabicyclodecanes were prepared in high yield with the creation of up to three stereocenters in a single pot by the acid-mediated reaction of γ,δ-unsaturated alcohols with aldehydes (see scheme, Bn=benzyl). This versatile reaction enables the stereoselective introduction of substituents at the C3, C4, C7, and C9 positions of the bicyclic framework. Copyright
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