Tetrahedron Letters p. 4671 - 4674 (1991)
Update date:2022-08-04
Topics:
Barton
Beviere
Doller
Treatment of alkanes under Gif(IV) conditions [FeCl2.4H2O (cat.), Zn0, and O2 in pyridine-acetic acid] in the presence of trimethylphosphite afforded alkyl dimethyl phosphates; 13C-NMR experiments showed that the phosphates are formed from the reaction between the intermediate alkyl hydroperoxide and trimethyl phosphite in the presence of an iron catalyst.
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