Tetrahedron Letters p. 7207 - 7210 (1991)
Update date:2022-08-03
Topics:
Schmittling, Elisabeth A.
Sawyer, J. Scott
The use of potassium fluoride on basic alumina in acetonitrile with ultrasound for the selecting deprotection of tert-butyldimethylsilyl ethers of phenols is described. The method, which features a non-aqueous work-up, readily cleaves tert-butyldimethylsilyl ethers of phenols at room temperature, whereas tert-butyldimethylsilyl ethers of benzyl alcohols or 2-(trimethylsilyl) ethoxymethyl ethers of phenols are stable.
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