Tetrahedron p. 913 - 922 (1992)
Update date:2022-08-03
Topics:
Keseru
Mezey-Vandor
Nogradi
Vermes
Kajtar-Peredy
Plagiochins C (3) and D (4) were synthesized by convergent schemes. Rings C and B were joined by Ullman ether synthesis, the aryl-aryl bond between rings A and D was formed by Pd(0)-catalysed coupling of an arylboronic acid (ring D) and a bromobenzoic ester (ring A). Rings C and D were linked by the Wittig reaction, while final ring closure was effected by tetraphenylethene assisted Wurtz reaction.
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