Angewandte Chemie - International Edition p. 11774 - 11777 (2012)
Update date:2022-08-03
Topics:
Barroso, Santiago
Castelli, Riccardo
Baggelaar, Marc P.
Geerdink, Danny
Terhorst, Bjorn
Casas-Arce, Eva
Overkleeft, Herman S.
Van Der Marel, Gijsbert A.
Codée, Jeroen D.C.
Minnaard, Adriaan J.
Complex: The synthesis of the glycolipid PGL-tb1 present in the outer membrane of hypervirulent strains of Mycobacterium tuberculosis has been accomplished for the first time by using a highly convergent strategy featuring a Sonogashira coupling to unite a phenolic trisaccharide with the phthiocerol. Efficient asymmetric Cu-catalyzed 1,4-additions to unsaturated thioesters and cyclic enones have been employed to introduce the methyl groups. Copyright
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Doi:10.3390/molecules171213856
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(2013)
