Synthesis of Vicinal Diamines by SmI2-Promoted Reduction of N-(N',N'-Dialkylaminoalkyl)benzotriazoles

DOI: 10.1016/S0040-4039(00)61280-7

Source and publish data:

Tetrahedron Letters p. 4763 - 4766 (1992)

Update date:2022-07-29

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Authors:

Aurrecoechea, Jose M.

Fernandez-Acebes, Alvaro

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Article abstract of DOI:10.1016/S0040-4039(00)61280-7

N-(N',N'-Dialkylaminoalkyl)benzotriazoles, derived from aldehydes and secondary amines, react with one equivalent of samarium iodide (SmI2), under mild conditions, to afford tertiary vicinal diamines, as a result of C-C coupling between two dialkylaminoalkyl moieties.

Full text of DOI:10.1016/S0040-4039(00)61280-7

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