Fluorinated ketene dithioacetals; 1. Preparation and application to the synthesis of α-trifluoromethylthiocarboxylic S-esters and aldehyde derivatives

DOI: 10.1055/s-1992-26280

Source and publish data:

Synthesis p. 965 - 968 (1992)

Update date:2022-08-02

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Authors:

Muzard Muzard

Portella

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Article abstract of DOI:10.1055/s-1992-26280

α-Trifluoromethylketene dithioacetals 3 were synthesized by Peterson reaction from trifluoromethyl ketones 1 and trimethylsilyl dithioacetals 2. Acid hydrolysis and reduction yield α-trifluoromethylthiocarboxylic S-esters 4 and α-trifluoromethyl dithioace

Full text of DOI:10.1055/s-1992-26280

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