Tetrahedron Asymmetry p. 101 - 108 (1993)
Update date:2022-08-04
Topics:
Rodriguez, Juan B.
Markey, Sanford P.
Ziffer, Herman
Optically pure samples of both enantiomers of methyl 2,3-dihydroxy-2-methylpropanoate were prepared by a chromatographic separation of their (-)-menthyl esters followed by hydrolysis and methylation.Their absolute stereochemistries were established by conversion into their 3-O-acetyl derivatives, compounds of established configuration.NMR and GC-MS methods of determining the optical purities of the diols are described.
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