Stereospecific Synthesis of (2R,3S)-3-Amino-2-Piperidineacetic Acid Derivatives for Use as Conformational Constraint in Peptides

DOI: 10.1016/S0040-4039(00)73644-6

Source and publish data:

Tetrahedron Letters p. 3593 - 3594 (1993)

Update date:2022-08-02

Topics:

Authors:

Gomez-Monterrey, Isabel

Gonzalez-Muniz, Rosario

Herranz, Rosario

Garcia-Lopez, Teresa

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Article abstract of DOI:10.1016/S0040-4039(00)73644-6

Catalytic hydrogenation at 40 deg C of the β-ketoester, obtained from Boc-Orn(Z)-OH and ethyl lithioacetate, provides exclusively ethyl (2R,3S)-3-tert-butyloxycarbonylamino-2-piperidineacetic acid which when suitably protected can be used for peptide synthesis.

Full text of DOI:10.1016/S0040-4039(00)73644-6

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Product name:ETHYL (2R, 3S)-3-BOC-AMINO-2-PIPERIDINEACETATE

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