A convenient synthesis of N-acetyllactosamine derivatives from lactal

DOI: 10.1016/0008-6215(93)84249-6

Source and publish data:

Carbohydrate Research p. 159 - 164 (1993)

Update date:2022-08-04

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Authors:

Toepfer Toepfer

Schmidt Schmidt

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Article abstract of DOI:10.1016/0008-6215(93)84249-6

In a thermal inverse-type hetero-Diels-Alder reaction of O-silyl-protected lactal 1 and bis(2,2,2-tri-chloroethyl) azodicarboxylate (2), the dihydrooxadiazine derivative 3 was obtained in a very high yield; transesterification with benzyl alcohol furnishe

Full text of DOI:10.1016/0008-6215(93)84249-6

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Product name:methyl O-(2,4,6-tri-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-tert-butyldimethylsilyl-2-deoxy-2-<1,2-di(benzyloxycarbonyl)hydrazino>-β-D-glucopyranoside

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