Chemical and Pharmaceutical Bulletin p. 277 - 279 (1994)
Update date:2022-08-05
Topics:
Jing
Shimada
Maeda
Arai
Goto
Aoyagi
Ohta
Astechrome (1), isolated from Aspergillus terreus IFO 6123 and 8835, was synthesized. Indolylmagnesium bromide (4) was coupled with a chloromethylpyrazine (5) to give 2-chloro-5-methoxy-3-methyl-6-[7-(3-methyl- 2-butenyl)indol-3-yl]methylpyrazine 1-oxide (6), which was converted to the Fe salt (9) of a hydroxamic acid derivative (8). Oxidation of 9 with (Co(salen) afforded 1.
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Doi:10.1007/s10593-014-1437-z
()Doi:10.1016/S0040-4020(01)85270-4
(1994)Doi:10.1021/ol500574b
(2014)Doi:10.1021/acs.jmedchem.6b00777
(2016)Doi:10.1016/j.jfluchem.2014.01.013
(2014)Doi:10.1021/ja500036r
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