Journal of Heterocyclic Chemistry p. 873 - 879 (1999)
Update date:2022-09-26
Topics:
Ishikura, Minoru
Agata, Isao
Katagiri, Nobuya
The palladium catalyzed cross-coupling reaction of indolylborates with various N-protecting groups was investigated, where N-Methyl, N-methoxy, and N-tert-butoxycarbonyl groups were found to be useful. However, triethyl(1-methoxymethylindol-2- yl)borate could not be used for this reaction. It was also found that the alkyl migration reaction of trialkyl(1- methoxymethylindol-2-yl)borate produced 2-alkyl-1-methyl-indole accompanied by the unexpected reduction of 1-methoxymethyl group to 1-methyl group.
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