Organometallics p. 1529 - 1532 (1995)
Update date:2022-07-29
Topics:
Liu, Shiuh-Tzung
Hou, Duen-Ren
Lin, Tu-Chen
Cheng, Ming-Chu
Peng, Shie-Ming
Reaction of o-C6H4(PPhH)(SH) (3) with Mn(CO)5Br and Re(CO)5Br in chloroform provided sulfido-bridged binuclear complexes {fac-[o-C6H4(PPhCl)(μ2-S)]Mn(CO) 3}2 (4) and [o-C6H4(PPhH)(μ2-S)](μ 2-Br)Re2(CO)7 (5), respectively. Both complexes 4 and 5 were characterized by spectral and crystal structural analyses. The hydrogen atom of the secondary phosphine moiety (P-H) of 3 was replaced by a chlorine atom in dimanganese complex 4 to form P-Cl but was retained in rhenium complex 5. Methanolysis of 4 gave methoxyl-substituted product {fac-[o-C6H4(PPh(OCH3))(μ 2-S)]Mn(CO)3}2.
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Doi:10.1021/ja5046814
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