Tetrahedron Letters p. 1709 - 1712 (1995)
Update date:2022-08-05
Topics:
Hassner, Alfred
Belostotskii, Anatoly M.
Action of triphenylphosphine - carbon tetrachloride on the trans-4-alkylaminocyclohexanols leads to 7-alkyl-7-azabicyclo[2.2.1]heptanes in the good yields. The starting aminoalcohols are easily available from the monoethylene ketal of 1,4-cyclohexanedione and primary amines in a four step process without isolation of intermediates.
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