Tetrahedron p. 9757 - 9766 (1995)
Update date:2022-08-04
Topics:
Lucchesini, Francesco
Bertini, Vincenzo
Pocci, Marco
De Munno, Giovanni
Crispini, Alessandra
The acid catalyzed acetalization of 2,6-bis(2-hydroxyethoxy)benzaldehyde (4) is studied under various conditions. New 2,3-dihydro-5H-1,4-benzodioxepin derivatives are prepared and a fourteen-membered tetraoxy-genated macrocycle is obtained in 81% yield without special synthetic expedients. The solid state molecular structure of the macrocyclic compound is determined by single crystal X-ray analysis.
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Doi:10.1021/jo990634s
(1999)Doi:10.1021/ja953060r
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(1995)Doi:10.1002/ardp.19743070805
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(1995)
