Australian Journal of Chemistry p. 1587 - 1600 (1995)
Update date:2022-08-05
Topics:
Hartshorn, Chris M.
Steel, Peter J.
Twelve new multidentate poly(pyrazol-1-ylmethyl)benzene ligands, (5)-(16), have benn synthesized by phase-transfer-catalysed alkylations of pyrazoles with poly(bromomethyl)benzenes, and their 1H and 13C n.m.r. spectra have been fully assigned.X-Ray crystal structure determinations have been carried out on the tetrachloropalladate salt of the diprotonated form of 1,4-bis(3,5-dimethylpyrazol-1-ylmethyl)-2,3,5,6-tetramethylbenzene and on hexakis(pyrazol-1-ylmethyl)benzene.
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