Tetrahedron p. 4645 - 4658 (1996)
Update date:2022-07-29
Topics:
Marty, Maurus
Stoeckli-Evans, Helen
Neier, Reinhard
While attempting to synthesize a potential inhibitor of the biosynthesis step of formation of PBG, a novel catalytic system inducing the Prins reaction was discovered. Treatment of epoxy geranial with Zn and trimethylsilyl chloride gave (1S,2S,3R,6S) 3-Chloro-3-methyl-6-isopropenyl-1,2-cyclohexanediol in high diastereoselectivity.
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(2017)
