α-Zinc O-vinyl carbamates as anionic Friedel-Crafts equivalents. Cross coupling reactions with aryl and heteroaryl halides and triflates

DOI: 10.1016/0040-4039(96)01314-7

Source and publish data:

Tetrahedron Letters p. 6057 - 6060 (1996)

Update date:2022-07-30

Topics:

Authors:

Superchi, Stefano

Sotomayor, Nuria

Miao, Guobin

Joseph, Babu

Snieckus, Victor

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Article abstract of DOI:10.1016/0040-4039(96)01314-7

A mild, efficient, and general Negishi cross coupling protocol, 4 + 5 → 6 is reported; the hydrolysis of products 6 to acetophenones demonstrates the anionic Friedel-Crafts equivalency of the overall synthetic operation.

Full text of DOI:10.1016/0040-4039(96)01314-7

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Product name:Diethyl-carbamic acid 1-(3-diethylcarbamoyl-phenyl)-vinyl ester

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