Synthesis of high-specific activity tritium and optically pure [14C]CP 101,606. Enantioselective crystallization of a radiochemically racemic mixture.

DOI: 10.1002/(SICI)1099-1344(199712)39:12<973::AID-JLCR40>3.0.CO;2-O

Source and publish data:

Journal of labelled compounds and radiopharmaceuticals p. 973 - 985 (1997)

Update date:2022-08-05

Topics: Optically pure Tritium

Authors:

McCarthy

Miller Miller

Chenard Chenard

Butler Butler

Dumont Dumont

Stemple Stemple

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Article abstract of DOI:10.1002/(SICI)1099-1344(199712)39:12<973::AID-JLCR40>3.0.CO;2-O

The syntheses of racemic, high-specific activity tritium and optically pure, carbon-14 labelled CP-101,606 is described. The tritium labelled material was prepared at 35.6 Ci/mmol by hydrogenolysis of the dibromo analog 5. In the carbon-14 synthesis, the

Full text of DOI:10.1002/(SICI)1099-1344(199712)39:12<973::AID-JLCR40>3.0.CO;2-O

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