Tetrahedron Asymmetry p. 759 - 763 (1997)
Update date:2022-07-30
Topics:
Delogu, Giovanna
Fabbri, Davide
Two new useful methods for the preparation of diol 1 starting from available compounds are described. Separation of the two enantiomers entails resolution of racemic diol 1 via the corresponding diastereomeric N-methylated phosphorothioamidates. Their separation by recrystallization followed by reduction afforded diol (aS)-1 and (aR)-1 in 100% and 72% ee, respectively.
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