One step preparation and 1,3-dipolar cycloadditions of (S)-5-hydroxymethyl-1-pyrroline N-oxide

DOI: 10.1016/S0957-4166(97)00042-6

Source and publish data:

Tetrahedron Asymmetry p. 1031 - 1037 (1997)

Update date:2022-08-02

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Authors:

Closa, Montserrat

De March, Pedro

Figueredo, Marta

Font, Josep

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Article abstract of DOI:10.1016/S0957-4166(97)00042-6

The cyclic nitrone 1b has been prepared in enantiomerically pure form by direct oxidation of L-(+)-prolinol with dimethyldioxirane. A complete diastereoface differentiation has been observed in the 1,3-dipolar cycloaddition reaction of this nitrone to several 1,2-disubstituted electron deficient olefins.

Full text of DOI:10.1016/S0957-4166(97)00042-6

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