Carbohydrate Research p. 271 - 277 (1997)
Update date:2022-08-03
Topics:
Moreau, Vincent
Norrild, Jens Chr.
Driguez, Hugues
The best yield for the synthesis of the title compound was obtained by nucleophilic displacement of the di-O-triflyl group in methyl tri-O-benzyl-4-O-triflyl-β-D-galactopyranoside by 2,3,4,6-tetra-O-acetyl-1-S-acetyl-1-thio-β-D-glucopyranose in HMPA in the presence of diethylamine. Under these conditions, the formation of unsaturated side products was decreased.
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(1967)Doi:10.1248/cpb.45.966
(1997)Doi:10.1080/07328309708007332
(1997)Doi:10.1021/jo991665q
(2000)Doi:10.1007/BF02495358
(1997)Doi:10.1002/chem.201405402
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