Tetrahedron Letters p. 4247 - 4250 (1997)
Update date:2022-07-29
Topics:
Makabe, Hidefumi
Tanaka, Akira
Oritani, Takayuki
(+)-4-Deoxygigantecin (1) was totally synthesized from enantiomerically pure (-)-muricatacin (3). Thus, 3 afforded the key intermediate 5 through a five-step reaction sequence, which was then converted to (+)-4-deoxygigantecin (1) via the formation of bis-tetnhydrofuran unit 11 and a coupling reaction with iodo lactone synthon 16.
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