Total synthesis of 1,3-dideoxynojirimycin

DOI: 10.1016/S0040-4039(97)10166-6

Source and publish data:

Tetrahedron Letters p. 8275 - 8278 (1997)

Update date:2022-08-05

Topics:

Authors:

Gryko, Dorota

Jurczak, Janusz

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Article abstract of DOI:10.1016/S0040-4039(97)10166-6

Addition of allyl bromide (5) to N-benzyl-N-carbobenzoxy-O-tert- butyldimethyl-D-serinal (4) afforded with high diastereoselectivity anti- adduct 6 which subsequently transformed into (2R,4S,5R)-1,3- dideoxynojirimycin (1).

Full text of DOI:10.1016/S0040-4039(97)10166-6

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Product name:Benzyl-[(1R,2S)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-triphenylsilanyloxy-pent-4-enyl]-carbamic acid benzyl ester

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