Russian Chemical Bulletin p. 1952 - 1955 (1997)
Update date:2022-08-03
Topics: Recrystallization Aldehyde Ketone TLC (thin-layer chromatography) FT-IR spectroscopy Condensation Reaction Schiff Base Primary Amine Solid-state reaction Melting Point Determination Mortar and pestle
Khrushcheva
Loim
Sokolov
A new preparative method for the synthesis of Schiff bases by the solid-state interaction of crystalline organic and organometallic aldehydes and amines is suggested. The possibility of direct synthesis of aldimines in the solid state from amine salts without isolation of the free amines is demonstrated.
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