Synthesis of 5-(β-D-ribofuranosyl)-pyridin-2-one: A 'deletion-modified' analogue of uridine

DOI: 10.1016/S0040-4039(97)00197-4

Source and publish data:

Tetrahedron Letters p. 1669 - 1672 (1997)

Update date:2022-08-04

Topics:

Authors:

Matulic-Adamic, Jasenka

Beigelman, Leonid

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1016/S0040-4039(97)00197-4

Pyridin-2-one C-nucleoside 2 was prepared using several different approaches. The most efficient pathway utilized the condensation of 2,3,5-tri-O-benzyl-D-ribono-1,4-lactone (4) and 2-(benzyloxy)-5-bromopyridine (5), followed by deoxygenation with Et₃SiH/BF₃·Et₂O and removal of the benzyl protecting groups.

Full text of DOI:10.1016/S0040-4039(97)00197-4

Products guided by the article

Product name:Acetic acid (3aR,4S,6R,6aR)-4-(6-bromo-pyridin-3-yl)-6-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl ester

Cas No:209974-04-9

R&D Labs maybe for 209974-04-9

Huangshan Honghui Pharm Technology Co., Ltd.(expird)

website:http://www.honghuichem.com

Contact:18855958372

Address:Qingshan Wan No.1,Nanyuan Kou,SheXian Huangshan City,Anhui Province
SINO Industries Company Limited(expird)

Contact:86-29-85369724

Address:No.111, Jiefang Road, Xi’an, China
Dezhou Longteng Chemical Co., Ltd.

website:http://www.sodium-methoxide.cn/

Contact:0086-18866052283

Address:Xinhua Industrial Zone, Dezhou City, Shandong Province, China
Shanggao Ruiya Fine Chemicals Co., Ltd

Contact:+86-795-2592103

Address:Xingguang Nanlu,Shanggao County Industry Park
Zhejiang Chemicals Import & Export Corporation

Contact:86-571-87043088

Address:No.37,Qingchun Road,Hangzhou,China

Relevant to this article

Doi:10.1016/S0040-4039(00)70394-7
(1964)
Doi:10.1016/S0040-4039(01)89976-7
(1967)
The preparation and structural characterisation of bis(N,N-diethyl-monothiocarbamato)complexes of cadmium and of the novel tetrameric complex [Et₄Zn₄(OSCNEt₂)₂(NEt ₂)₂]: Two new bonding modes for the monothiocarbamato ligand

Doi:10.1039/a805986a
(1998)
Versatile route to functionalized 1H-2-benzothiopyrans and 1H-2- naphthothiopyrans by electrophilic cyclization of Bis(arylmethylthio)acetylenes: 2-Benzo- and 2-naphthothiopyrylium salts

Doi:10.1021/jo972334l
(1998)
Oxidative Rearrangement of Isatins with Arylamines Using H₂O₂ as Oxidant: A Facile Synthesis of Quinazoline-2,4-diones and Evaluation of Their Antibacterial Activity

Doi:10.1002/cjoc.201700280
(2017)
Syntheses of thiol and selenol esters by oxidative coupling reaction of aldehydes with RYYR (Y = S, Se) under metal-free conditions

Doi:10.1039/c4ob01159g
(2014)

Article Doi