Chemistry Letters p. 739 - 740 (1998)
Update date:2022-08-05
Topics:
Ohira, Susumu
Yoshihara, Naoya
Hasegawa, Taisuke
A spiro sesquiterpene alcohol, (-)-gleenol (1) was synthesized from (-)-1-menthol in 16 steps, using the C-H insertion reaction of the alkylidenecarbene as the key step. The absolute configuration of (-)-1 was determined to be IS, 6R, 7S. 10R.
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