Tetrahedron Letters p. 7193 - 7196 (1998)
Update date:2022-08-03
Topics:
Svensson, Anette
Bergquist, Karl-Erik
Fex, Tomas
Kihlberg, Jan
Three fluorinated linkers which are analogues of linkers commonly used in solid-phase peptide synthesis have been prepared. Using 19F NMR spectroscopy, the fluorine atom of the linker allowed monitoring of several transformations in the solid-phase synthesis of a peptoid having a coumarin moiety. Especially, attachment of the linker to the solid phase, coupling of the first building block to the linker and cleavage of the product were efficiently monitored and optimised.
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