Tetrahedron Letters p. 7471 - 7474 (1998)
Update date:2022-08-03
Topics:
Chow, Chun P.
Berkman, Clifford E.
N-Phosphoryl amino acids were prepared rapidly and in high yield via phosphoramidite amine-exchange in the presence of 1H-tetrazole followed by oxidation with mCPBA. Formation of dibenzyl phosphoramidates incorporating the representative C-terminal protected amino acids leucine, phenylalanine, glutamic acid, and proline were demonstrated to be most successful with dibenzyl N,N-dimethylphosphoramidite although the N,N-diethyl and N,N- diisopropyl analogs also provided high yields.
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Doi:10.1016/j.tet.2019.01.060
(2019)Doi:10.1016/S0040-4020(98)00777-7
(1998)Doi:10.1021/jo981279t
(1998)Doi:10.1021/jo980749g
(1998)Doi:10.1016/S0040-4039(98)01711-0
(1998)Doi:10.1016/S0039-128X(98)00060-9
(1998)
