Journal of the Chemical Society. Perkin transactions I p. 289 - 294 (1996)
Update date:2022-08-03
Topics:
Barbero, Margherita
Degani, Iacopo
Dughera, Stefano
Fochi, Rita
Piscopo, Laura
1,3-Dithiolan-2-ones have been obtained by reaction of 1,3-dithiolane-2-thiones and epoxides in the presence of HBF4·Et2O. The reactions, carried out in anhydrous CH2Cl2 at 0-5°C→room temperature (Procedure A) or in anhydrous chlorobenzene at 0-5→80°C (Procedure B), gave product yields of 63-95%. By Procedure B it was also possible to isolate the intermediates 1-oxa-4,6,9-trithiaspiro[4,4]nonanes in good yields (66-85%). Reaction pathways are proposed.
View MoreContact:86-15588110016
Address:LINYI CITY,SHANDONG PROVINCE,CHINA
Buffett (China) Holding Co.,Ltd
Contact:4006570891
Address:
Contact:0792-8228321
Address:10TH Floor No.121 binjiang Road Xunyang District
Chongqing Shuangfeng Chemical Co.,Ltd
Contact:+86-23-49850156
Address:No.663,xuanhua Rd,yongchuan,chongqing,China
Beijing Tianjia Chemical Science & Technology Co.,Ltd
Contact:86-0550-2392698
Address:No.388, Shiliang Road (East),
Doi:10.1007/BF00486781
()Doi:10.1002/(SICI)1099-0682(199810)1998:10<1563::AID-EJIC1563>3.0.CO;2-P
(1998)Doi:10.1021/ja01205a506
(1946)Doi:10.1039/P19730000083
(1973)Doi:10.1016/S0031-9422(97)00949-7
(1998)Doi:10.1021/jo01278a065
(1967)
