Tetrahedron Letters p. 977 - 980 (1999)
Update date:2022-07-29
Topics:
Wang, Zhi-Min
Tian, Shi-Kai
Min, Shi
A highly efficient synthetic method for the trans/threo/trans- bis- tetrahydrofuran (THF) ring building block was established. The title compound was synthesized in thirteen steps from trans-1,4-dichloro-2-butene via a convergent route with a Wittig reaction as the key step. The absolute configuration of the THF segment of naturally occurring asimilobin should be corrected.
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