Tetrahedron Letters p. 9005 - 9007 (1999)
Update date:2022-08-02
Topics:
Gautheron Chapoulaud
Audoux
Ple
Turck
Queguiner
We describe a multistep synthesis leading in a good yield to the title compound. The biaryl linkage was formed in a Pd-catalysed coupling of 2-phenyl-4-chloroquinazoline with 2-methoxy-1-naphthylboronic acid. A further metal-catalysed reaction gave the formation of the naphthylphosphorus bond allowing us to obtain the required phosphonimine ligand 1 as the racemate.
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