Total Syntheses of Squamocin A and Squamocin D

DOI: 10.1016/S0040-4039(99)01225-3

Source and publish data:

Tetrahedron Letters p. 5979 - 5982 (1999)

Update date:2022-08-04

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Authors:

Emde, Ulrich

Koert, Ulrich

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Article abstract of DOI:10.1016/S0040-4039(99)01225-3

The total syntheses of two acetogenins, squamocin A and squamocin D, have been achieved. The adjacent bis-THF subunit was constructed by a multiple Williamson reaction. The left and the right side chain were added by addition of organomagnesium compounds to aldehyde functions. The conversion of a carboxylic acid into the butenolide moiety concluded both syntheses.

Full text of DOI:10.1016/S0040-4039(99)01225-3

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