Tetrahedron p. 12983 - 12990 (1999)
Update date:2022-09-26
Topics:
Kim, Dae Young
Lee, Yong Mi
Choi, Young Jae
Acylation of α-fluorophosphonoacetate derivatives in the presence of magnesium chloride-triethylamine has been described. Acylations of triethyl α-fluorophosphonoacetate 1 and diethyl α-fluorophosphonoacetic acid 7 were proceeded under mild conditions to provide α-fluoro-β-keto esters 3 and α- fluoro-β-keto phosphonates 9, respectively, in high yields.
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