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1
2
2
[60] Rw(F2) = {w(jFo j À jFc j )2/w(jFo j)4} = where w is the weight given
2
each reflection. R(F) = (jFo j À jFc j)/jFo j} for reflections with Fo
>
1
2
2
4((Fo)). S = [w(jFo j À jFc j )2/(nÀp)] = , where n is the number of
reflections and p is the number of refined parameters.
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2
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Received: November 20, 2003
Revised: March 4, 2004
Published online: June 21, 2004
3804
¹ 2004 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim
Chem. Eur. J. 2004, 10, 3792 3804