
Tetrahedron Letters p. 5135 - 5138 (1981)
Update date:2022-08-05
Topics:
Mitchell, Reginald H.
Anker, Willem
The synthesis of syn- and anti-9-methyl-18-phenyl- and anti-9,18-diphenyl-2,11-dithia<3,3>metacyclophanes is described, together with their variable temperature 1Hmr spectra.Only partial rotation of the phenyl substituents (ΔG<*>c<*>50 kJ./mol) is believed to occur.
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Doi:10.1007/BF00471473
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(1971)