Tetrahedron Letters p. 3225 - 3228 (1999)
Update date:2022-08-02
Topics:
Guellue, Mustafa
Electrochemical cyclisation of methyl cinnamate with dielectrophiles has been improved by the presence of an aluminum salt which was pre-formed in situ by the electrolysis of a carboxylic acid with a sacrificial aluminum anode. High yields of three, five and six-membered cyclic products have been obtained in the reactions of methyl cinnamate with dichloromethane, 1,3- dibromopropane, and 1,4-dibromobutane.
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