Synthetic Communications p. 2661 - 2666 (2006)
Update date:2022-08-02
Topics:
Zhou, Yuhan
Gong, Runjun
Miao, Weirong
N-Chloroformyl-N-arylcarbamate, the key intermediate for the synthesis of some excellent pesticides, was synthesized through a new method with triphosgene instead of toxic phosgene. It cannot be obtained through the traditional method using triethylamine as a nucleophile. When triethylamine was replaced by a stronger base, sodium hydride, the product was obtained in good yield. Copyright Taylor & Francis Group, LLC.
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