Russian Chemical Bulletin p. 1991 - 1994 (1993)
Update date:2022-08-03
Topics:
Polivin, Yu. N.
Karakhanov, R. A.
Kelarev, V. I.
Sheveleva, T. S.
Ugrak, B. I.
The reaction of methylmagnesium iodide with di(n-butyl)cyanamide results in dibutylamine, dibutylisopropylamine, and acetonitrile, while the reaction with di(n-butyl)nitrosamine affords acetaldehyde dibutylhydrazone.Formaldehyde, acetone, and 2-butanone dibutylhydrazones, as well as acetaldehyde butyl(1-methylbutyl)hydrazone, 2-butanone butyl(1-methylbutyl)hydrazone, 1,1-dibutyl-2,2-dimethylhydrazone, and 1,1-dibutyl-2-ethyl-2-methylhydrazine were also identified in minor amounts.Di(n-butyl)nitramine reacts with methylmagnesium iodide to give di(n-butyl)nitrosamine. - Key words: di(n-butyl)cyanamide; di(n-butyl)nitrosamine; methylmagnesium iodide; formaldehyde dibutylhydrazone; 2-butanone dibutylhydrazone; acetaldehyde butyl(1-methylbutyl)hydrazone; 2-butanone butyl(1-methylbutyl)hydrazone; 1,1-dibutyl-2,2-dimethylhydrazine; 1,1-dibutyl-2-ethyl-2-methylhydrazine; di(n-butyl)nitramine.
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