
Journal of labelled compounds and radiopharmaceuticals p. 141 - 148 (1978)
Update date:2022-08-02
Topics:
Harrison
Inch
Lawston
Ley
Sainsbury
Using similar procedures, the syntheses of [2-14C]-malononitrile and malono [14C]nitrile are described. Condensation with o-chlorobenzaldehyde affords [2-14C]-o-chlorobenzylidenemalononitrile and o-chlorobenzylidenemalono [14C]nitrile respectively. The syntheses of [3H]o-chlorobenzaldehyde and o-chlorobenz[ 14C]aldehyde, again by a common sequence of reactions, is described and with malononitrile gives [3H]-o-chlorobenzylidenemalononitrile and [1-14C]-o-chlorobenzylidenemalononitrile.
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Doi:10.1021/ja00481a011
(1978)Doi:10.1016/S0040-4039(00)96822-9
(1987)Doi:10.1039/jr9490002620
(1949)Doi:10.1016/j.bmcl.2003.11.061
(2004)Doi:10.1016/j.tetlet.2004.03.151
(2004)Doi:10.1039/c7cc09926f
(2018)