Synthetic Communications p. 3218 - 3225 (2019)
Update date:2022-08-05
Topics:
Wu, Caijiao
Li, Hui
Sun, Feiyang
Bao, Changshun
Bao, Xuefei
Chen, Guoliang
A synthetic route to the precursor of FP- (+) DTBZ was disclosed, in which 3-hydroxy-4-methoxybenzaldehyde was employed as a starting material. In the method, the benzyl-protecting protocol and the in-situ Diels-Alder reaction made the procedure more practical because of the mild conditions for selectively deprotection and the accelerated reaction process.
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