Tetrahedron Letters p. 2707 - 2710 (1990)
Update date:2022-08-03
Topics:
Horeau
Nouaille
An optically active secondary alcohol is treated by an equimolecular mixture of (+)-2-phenylbutyric and (-)-2-phenyl-4-d-butyric anhydrides. The configuration of the carbon atom bearing the OH group is deduced from the relative heights of peaks m/z 120 and 119 observed in the mass spectra of the resulting diastereoisomeric esters.
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