Tetrahedron Letters p. 1933 - 1936 (1981)
Update date:2022-08-05
Topics:
Jones, Simon S.
Reese, Colin B.
Sibanda, Samson
Alcohols (ROH) may be converted into their MTMEC derivatives (6) by acylation with 2-(methylthiomethoxy)ethoxycarbonyl chloride (5); the MTMEC "protected protecting group" may be removed by treatment first with Hg(II) perchlorate in the presence of 2,4,6-collidine or pyridine in aceton-water solution, followed by hydrolysis under very mild basic conditions.
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