Tetrahedron Letters p. 1933 - 1936 (1981)
Update date:2022-08-05
Topics:
Jones, Simon S.
Reese, Colin B.
Sibanda, Samson
Alcohols (ROH) may be converted into their MTMEC derivatives (6) by acylation with 2-(methylthiomethoxy)ethoxycarbonyl chloride (5); the MTMEC "protected protecting group" may be removed by treatment first with Hg(II) perchlorate in the presence of 2,4,6-collidine or pyridine in aceton-water solution, followed by hydrolysis under very mild basic conditions.
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Doi:10.1021/ja00535a043
(1980)Doi:10.1002/anie.201303831
(2013)Doi:10.1248/cpb.28.235
(1980)Doi:10.1021/ja01133a512
(1952)Doi:10.1039/c1dt11249j
(2011)Doi:10.1016/S0040-4039(02)02862-9
(2003)
