Journal of Organometallic Chemistry p. 93 - 104 (1980)
Update date:2022-08-05
Topics:
Patin, Henri
Mignani, Gerard
Mahe, Christian
Marouille, Jean-Yves Le
Benoit, Alain
Grandjean, Daniel
Ferrocenyltrithiocarbonates (I) are readily obtained by treating α-ferrocenylcarbinols (II) successively with sodium hydride, carbon disulfide and alkyl halide.Formation of I occurs by intramolecular nucleophilic displacement of oxygen by sulfur with retention of configuration.This is supported by the nature of the other products formed and by the X-ray structure determination of an optically active compound I, which was refined to R = 0.038.The title compound of R configuration was obtained from (R)-ferrocenylmethylmethanol.
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