Tetrahedron p. 1109 - 1111 (1983)
Update date:2022-07-29
Topics:
Bergmark, William R.
Meador, Michael
Isaacs, James
Thiim, Michael
The title compound was prepared and irradiated under a variety of conditions to produce no change.Irradiation id DMSO-d6 and methanol-d4 results in D incorporation into the o-(trimethylsilyl)methyl group.Irradiation in 2-propanol results in photoreduction (φ=0.012) which could be quenched with dienes (kqτ=4.5).These results are taken to suggest a rapid, efficient, and reversible H-transfer with no detectable silyl transfer.
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