Journal of the Chemical Society. Chemical communications p. 675 - 676 (1981)
Update date:2022-08-04
Topics:
Lown, J. William
Chauhan, Shive M. S.
Nitrosothioureas may be prepared by treatment of thioureas with NaNO2 in 0.1 N HCl at -5 deg C by direct N-nitrosation whereas 15N n.m.r. studies at -10 deg C which employed specifically 15N-enriched compounds revealed the intermediacy of a thionitrosyl compound under more acidic conditions which gave the urea by hydrolysis.
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