Synlett p. 1308 - 1310 (2001)
Update date:2022-08-05
Topics:
Funabiki
Fukushima
Sugiyama
Shibata
Matsui
Abstract: 1-Aryl-substituted 2,3,3-trifluoro-1-propenyl p-toluene-sulfonate 1 was smoothly hydrolyzed in a mixed solvent of dimethyl sulfoxide-water (1:1) in the presence of sodium hydroxide at 80 °C to afford the corresponding aryl α-monofluoromethyl ketones 2 in fair to good yields.
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Doi:10.1021/jo00423a049
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